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Beilstein J. Org. Chem. 2015, 11, 1815–1822, doi:10.3762/bjoc.11.197
Graphical Abstract
Figure 1: Structures of (−)-zampanolide (2) and (+)-dactylolide (3).
Scheme 1: Retrosynthesis of zampanolide involving a Bestmann ylide linchpin strategy.
Scheme 2: Synthesis of aldehyde 8.
Scheme 3: Bestmann ylide linchpin coupling of the C16–C20 and C3–C8 fragments of zampanolide/dactylolide.